Control of the crystallization front shape in the course of large CsI(Na) single crystals growing by Kyropoulos automated method

V.I.Goriletsky


Institute for Single Crystals, National Academy of Ukraine, 60 Lenin Ave., 310001 Kharkiv, Ukraine

Received September 25, 1998

The causes of diameter variations of the crystal being grow by Kyropolous method have been considered at the initial stage of longitudinal crystal growth with automated mass control of the crystallizing melt. It has been shown that when crystals over 300 mm diameter are grown, the local changes of the front shape are the main cause of considerable diameter variations. There changes are due to jump-like changes of heat-exchange conditions between the crystal surface and the environment, and those, in turn, result in structural, optical and other defects in the crystal. The technique for process control to prevent the above-mentioned effect is proposed. A particular case of single crystal growing without pulling from melt is described (automated method by Kyropolous).

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