Funct. Mater. 2016; 23 (1): 005-014.

http://dx.doi.org/10.15407/fm23.01.005

Perspectives of development of X-ray analysis for material composition

I.F.Mikhailov, A.A.Baturin, A.I.Mikhailov, L.P.Fomina

National Technical University "Kharkiv Polytechnical Institute", 21 Frunze Str., 61002 Kharkiv, Ukraine

Abstract: 

Perspectives are considered for increasing the sensitivity of X-ray analysis and broadening the range of measurements toward chemical elements with small atomic numbers up to hydrogen at the expense of formation of the optimized selective spectrum from a preliminary beam for exciting fluorescence and observing scattering peaks and diffraction reflections. It has been shown that low-power preliminary sources (X-ray tube, 20 W) are able to provide the detection limit for trace impurities near 0.1 ppm, and for hydrogen in metals - up to 10 ppm. The data presented are hopeful for attaining X-ray analysis sensitivity at the level of ppb units due to application of powerful preliminary beams (synchrotron, undulators, wigglers, etc.).

Keywords: 
X-ray analysis, Compton scattering, X-ray spectrometers.
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