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Funct. Mater. 2019; 26 (2): 381-383.

doi:https://doi.org/10.15407/fm26.02.381

A novel gas chromatography analysis nethod of acryloyl chloride

Qihui Shen, Xinchen Xu, Yang Lu, Miao Li, Yan Liu

Department of Chemistry and Pharmaceutical Engineering, Jilin Institute of Chemical Technology, 45 Chengde Str., 132022 Jilin, P. R. China

Abstract: 

A novel method for the determination of acryloyl chloride in industrial products by aniline derivatization and gas chromatography is described. In this method, ethyl acetate was used as solvent but not toluene or benzene. The precision and recovery of this method were 0.474 % - 1.64 % and 95.3 - 98.2 %, respectively and up to the analysis standard. And the method had achieved non-irritation and non-corrosive.

Keywords: 
gas chromatography, acryloyl chloride, derivatization.
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